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Beilstein J. Org. Chem. 2018, 14, 642–647, doi:10.3762/bjoc.14.51
Graphical Abstract
Scheme 1: SET-triggered Diels–Alder reaction of trans-anethole (1) and isoprene (2).
Figure 1: Plausible mechanism for the electrocatalytic Diels–Alder reaction. Adapted from [22].
Scheme 2: Undesired dimerization of trans-anethole (1).
Figure 2: GC–MS monitoring of the electrocatalytic Diels–Alder reaction (1: 300 mM; 2: 3000 mM).
Figure 3: GC–MS monitoring of the electrocatalytic Diels–Alder reaction (1: 1 mM; 2: 2000 mM).
Figure 4: GC–MS monitoring of the electrocatalytic Diels–Alder reaction (1: 2 M; 2: 6 M). Blue dots show the ...